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Double Glass Reactor Introduction

Nanjing Xianou manufacturing double glass reactor  with double deck glass design,input the reaction solvent into the inner layer could be stirring. And the interlayer connects with various hot or cold source (eg: refrigerating fluid, hot water or hot oil) so that can do cyclic heating or cooling reactions. Under the condition of setting constant temperature, in the sealed glass reactor, enable to do stirring reactions in ordinary pressure or negative pressure situation according to experimental requirements, and reacting solution could be distilled and back flowed. This type reactor is the ideal pilot production equipment for modern fine chemicals, biopharming and synthesis of new materials.

 

Double glass reactor operating instruction:


1. Check whether the power supply voltage and the specifications machine nameplate provides are consistent.


2.Plug plugged, open the inverter power supply switch,and choose suitable for speed with speed control knob.


3.Material flow and the power of the motor speed may cause resonance at some point, please change the speed of motor to avoid resonance.


4.After mounting muddler, must make a rotating with hand , pay attention whether concentricity is fine, such as bad concentricity should loosen the heavy clip, after right clipping,turn on the power supply, adjusting gradually from slowly to quickly .


5.Using muddler regulator,stirring leaf can fluctuate 5 cm according to the need.

 

Key Features:


1.Whole unit with stainless steel column movable frame construction, five front-openings reactor lid, mating with full set of glass: back flowing, liquid adding and temperature measuring;


2.Use GG17 borosilicate glass, have a good chemical and physical properties;


3.Alloy steel mechanical seals, Teflon connectors, keep high-precision sealing under the working state;


4.With Pt100 sensor probe, temperature measurement with high precision, small error and effectively improve the work efficiency;


5.Japan technology exchange Gear Reducer Motor, strong torque, no noise;


6.Pairs of Teflon stirring paddle, suitable for low or high viscosity fluid mixing and stirring.

 

Technology Parameters:

 

Model

Capacity

Motor Power

Speed

(rpm)

Torque

(1300r/min)

In/Out Tube Diameter

The Related Opening of Glass Reactor

Dimension

 

(L)

 

 

 

(mm)

Center

Left

Right

Behind

Front

(cm)

XO-1L

1

40W

100-1300

2400.g.cm

150*180

50#

29#

24#

----

14#

35*27*60

XO-2L

2

90W

100-1300

5000g.cm

150*180

50#

29#

24#

----

14#

44*32*84

XO-3L

3

90W

100-1300

5000g.cm

200*230

50#

29#

24#

----

19#

44*32*84

XO-5L

5

90W

100-1300

5000g.cm

200*230

50#

29#

24#

24#

19#

44*32*84

 

COMMON ISSUES&SOLUTIONS:

 

Phenomenon

Reasons

Remove

Turning on  the power swith,the indicator light inoperative 

Not connected external power supply or bad contacting

Inviting professional electrician to check the power supply and socket.

 

 

Power light lighting,but nonrotating 

The axis is rusted.

Stop using, and contact with supplier

Motor or electrical box break down

Not connected seven core plugs

Connecting seven core plugs again

Vacuum disappearing suddenly 

Glass has a crack, or switch is damaged.

Check glass parks,and exchange switch.

Vacuum,but no pumping 

Sealing ring wear, connecting vacuum switch leaking

 

Please exchange sealing ring and switch.

Vacuum coming and going

Steel shaft is dirt, connectors  have loose.

 

Please remove dirt and check vacuum meter ,vacuum pump.  

Vacuum hose aging

Please exchange vacuum hose.

Main machine core shaft loosing

Tight top screw loose

Screwing 

Motor temperature too high(Adding 40℃ room temperature is normal)

Overload

Stop and turn machine pivot with hand.If it's very heavy, clear the dirt away on the contract of  sealing ring with glass shaft, coating vacuum fat

 

 

Speed show and the actual discrepant

Voltage is not stable,and their own has errors.

Contracting with supplier

Shell charged

Heating tube have crack,flooding water.

Inviting professional electrician to check

 

How to Maintenance of Glass Reactor:

1. Check instrument carefully with glass reactor,observing whether glass bottles have any breakage and The interface is identical.Pay attention to putting up and down with gentle.

 

2. Each interface of glass reactor cannot twist too tight,should loosen  periodically to avoid connector bite deadly due to long time locking.

 

3. Firstly turn on the power switch,then operating instrument from slowly to fastly.When stopping the instrument,make it in stopping state,at last turn off the switch.

 

4. Wipe the interface with soft cloth,then daub a little vacuum fat.
 

5. After downtime,unscrew the ptfe switch,it will make teflon piston deformation in the work of the state for long-term static.  
 

 

6.Cleaning sealing ring regularly,the method is that turn down sealing ring,check whether the shaft is dirty,if so,wipe clean with soft cloth, then daub a little vacuum fat. Mounting again,keep the shaft and sealing ring smooth.  

 

7.All ptfe switch can not quite tighten, otherwise it is easy to damage glass.

 

8.Must purchase original authentic accessories,it can cause fatal damage for using other accessories to machine at will.

 

9.Every time after using glass reactor,must wipe up all kinds of oil stains,blot,and remain solvent on the surface to keep clean. 

 

10.Electrical parts must have no water,and it is strictly prohibited to damp.